1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

Base Information

Chemical Name:1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne
CAS No.:1238279-09-8
Molecular Formula:C₃₇H₄₂N₄O₈S₃
Molecular Weight:766.96
Hs Code.:

Synonyms:1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

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Chemical Property of 1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

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Technology Process of 1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

There total 1 articles about 1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 700868-16-2
N-(4-bromo-2-butynyl)-N-(tert-butyloxycarbonyl)(4-methylphenyl)sulfonamide

: 1238279-18-9
N,N'-bis[(4-methylphenyl)sulfonyl]-N'-(2-cyanoethyl)-2-butyne-1,4-diamine

: 1238279-09-8
1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

Guidance literature:: With potassium carbonate; In acetonitrile; for 8h; Reflux;
DOI:10.1002/ejoc.200901318

Reference yield: 93.0%

: 1238279-09-8
1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

: 1238279-19-0
C₃₇H₄₂N₄O₈S₃

Guidance literature:: With Wilkinson's catalyst; In toluene; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.200901318

Reference yield: 91.0%

: 1238279-09-8
1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

: 1238279-10-1
1-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne

Guidance literature:: 1-(tert-butyloxycarbonyl)-11-(2-cyanoethyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diyne; With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere; Sealed tube;

With methanol;
DOI:10.1002/ejoc.200901318