dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)

Base Information

Chemical Name:dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)
CAS No.:173725-62-7
Molecular Formula:C₂₆H₃₇O₂PW
Molecular Weight:596.402
Hs Code.:

Synonyms:dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)

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Chemical Property of dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)

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Technology Process of dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)

There total 1 articles about dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 154293-83-1
dicarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenyl-λ(4)-phosphanediyl]tungsten(II)

: 74-88-4
methyl iodide

: 173725-62-7
dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](methyl)-λ(4)-phosphanediyl)tungsten(II)

Guidance literature:: With KO(t)Bu; In tetrahydrofuran; byproducts: t-BuOH, KI; N2-atmosphere; addn. of equimolar amt. of KO(t)Bu to W-complex soln. (0°C), then addn. of excess of MeI; solvent removal (vac.), dissoln. in pentane, chromy. (Al2O3, pentane), evapn. (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00947-4