(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Base Information

Chemical Name:(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid
CAS No.:918304-73-1
Molecular Formula:C₂₄H₃₅BO₄Si
Molecular Weight:426.436
Hs Code.:

Synonyms:(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Suppliers and Price of (3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

There total 2 articles about (3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918305-09-6
C₂₄H₃₃BrO₂Si

: 918304-73-1
(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Guidance literature:: C₂₄H₃₃BrO₂Si; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 17h; Further stages.;
DOI:10.1039/b609604b

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 121-43-7,63156-11-6
Trimethyl borate

: 13154-24-0
triisopropylsilyl chloride

: 10028-15-6
ozone

: 217493-10-2
(+/-)-3-ethenyl-7-bromo-3-phenyl-2,3-dihydrobenzofuran

: 918304-73-1
(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

Guidance literature:: With 1H-imidazole; n-butyllithium; oxygen; In tetrahydrofuran; CH2CHC8H5O(C6H5)Br reacted with O3 in CH2Cl2 at -78°C, reacted with O2-MeOH, reacted with NaBH4, reacted with Si compd. and imidazole in DMF, reacted with n-C4H9Li and B(OCH3)3 in THF;
DOI:10.1039/b609604b

Reference yield: 80.0%

: C₁₅H₁₉BrN₂O₂

: 918304-73-1
(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)boronic acid

: {2-[-4-(3-phenyl-3-triisopropylsilanyloxymethyl-2,3-dihydrobenzofuran-7-yl)-1H-indol-3-yl]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; for 17h; Heating;
DOI:10.1039/b609604b