C₂₅H₂₃IO₅

Base Information

• Chemical Name: C₂₅H₂₃IO₅
• CAS No.: 1110618-59-1
• Molecular Formula: C₂₅H₂₃IO₅
• Molecular Weight: 530.359
• Mol file: 1110618-59-1.mol

Synonyms:C₂₅H₂₃IO₅

Chemical Property of C₂₅H₂₃IO₅

Chemical Property:

Purity/Quality:

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Technology Process of C₂₅H₂₃IO₅

There total 1 articles about C₂₅H₂₃IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

benzyl bromide (100-39-0) + 3-(1,3-dioxan-2-yl)-2-hydroxy-5-iodobenzoic acid (685870-22-8) → C25H23IO5 (1110618-59-1)

Guidance literature:

3-(1,3-dioxan-2-yl)-2-hydroxy-5-iodobenzoic acid; With potassium carbonate; In acetone; for 0.5h;

benzyl bromide; In acetone; Reflux;

DOI:10.1039/b815099k

Reference yield: 68.0%

C25H23IO5 (1110618-59-1) + 1,4-bis(dodecyloxy)-2,5-diethynylbenzene (152270-00-3) → C84H98O12 (1110618-65-9)

Guidance literature:

With copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 18h;

DOI:10.1039/b815099k

upstream raw materials:

benzyl bromide

3-(1,3-dioxan-2-yl)-2-hydroxy-5-iodobenzoic acid

Downstream raw materials:

C₈₄H₉₈O₁₂

Refernces