1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

Base Information

Chemical Name:1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene
CAS No.:201035-87-2
Molecular Formula:C₃₁H₃₃NO₂Si
Molecular Weight:479.694
Hs Code.:

Synonyms:1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

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Technology Process of 1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

There total 1 articles about 1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 40400-15-5
2-(2-iodophenyl)acetonitrile

: tert-Butyl-diphenyl-[3-(5-tributylstannanyl-furan-2-yl)-propoxy]-silane

: 201035-87-2
1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; Heating;
DOI:10.1016/S0040-4039(97)10437-3

Reference yield: 75.0%

: 201035-87-2
1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

: 944382-73-4
1-[5'-(3''-hydroxy-propan-1''-yl)-2'-furanyl]-2-methylcyano-benzene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/S0040-4039(97)10437-3

Reference yield:

: 201035-87-2
1-[5-'-(3''-tert-butyldiphenylsilyloxy-propan-1''-yl)-2'-furanyl]-2-methylcyanobenzene

: 944382-56-3
1-[5'-(3''-bromo-propan-1''-yl)-2'-furanyl]-2-methylcyano-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / tetra-n-butylammonium fluoride; p-toluenesulphonic acid / tetrahydrofuran / 12 h / 0 - 20 °C

2: 85 percent / triphenylphosphine; carbon tetrabromide / CH₂Cl₂ / 0.5 h / 0 °C

With carbon tetrabromide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b703373g