trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

Base Information

Chemical Name:trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene
CAS No.:149754-09-6
Molecular Formula:C₃₁H₄₄NiO₃P₂
Molecular Weight:585.326
Hs Code.:

Synonyms:trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

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Chemical Property of trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

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Technology Process of trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

There total 1 articles about trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 111662-43-2
P-(pentamethylcyclopentadienyl)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 149754-09-6
trans-η1-P-(pentamethylcyclopentadienyl)(η1-tricarbonylnickel)-P'-(2,4,6-tri-t-butylphenyl)diphosphene

Guidance literature:: In diethyl ether; Ni(CO)4 was added (by a syringe) to a soln. of the diphosphene in Et2O and the mixt. stirred for 1 h;; after removal of all volatile compds. in vac., the black residue was recrystd. repeatedly from n-hexane at -30°C; elem. anal.;;
DOI:10.1016/0022-328X(92)85093-C