(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

Base Information

Chemical Name:(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide
CAS No.:1067185-73-2
Molecular Formula:C₃₄H₃₈O₃P*I
Molecular Weight:652.552
Hs Code.:

Synonyms:(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

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Chemical Property of (2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

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Technology Process of (2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

There total 1 articles about (2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1067185-78-7
(4S,6R)-4-benzyloxymethyl-6-(2-iodoethyl)-2,2-dimethyl-1,3-dioxane

: 603-35-0
triphenylphosphine

: 1067185-73-2
(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 22h; Heating;
DOI:10.1016/j.tetlet.2008.07.022

Reference yield: 17.0%

: 1067185-73-2
(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

: 1067185-71-0
(4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde

: 1067185-80-1
(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

Guidance literature:: (2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide; With potassium hexamethylsilazane; In toluene; at -78 ℃; for 0.5h;

(4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde; In toluene; at 20 ℃; for 2.5h; Further stages.;
DOI:10.1016/j.tetlet.2008.07.022