(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane
CAS No.:1067185-80-1
Molecular Formula:C₄₁H₅₆O₆Si
Molecular Weight:672.978
Hs Code.:

(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

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Chemical Property of (2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

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Technology Process of (2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

There total 2 articles about (2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1067185-73-2
(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide

: 1067185-71-0
(4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde

: 1067185-80-1
(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

Guidance literature:: (2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethyl)triphenylphosphonium iodide; With potassium hexamethylsilazane; In toluene; at -78 ℃; for 0.5h;

(4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde; In toluene; at 20 ℃; for 2.5h; Further stages.;
DOI:10.1016/j.tetlet.2008.07.022

Reference yield:

: 1067185-72-1
5-(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethylsulfonyl)-1-phenyl-1H-tetrazole

: 1067185-71-0
(4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde

: 1067185-80-1
(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

: 1067185-79-8
(2-((4S,6S)-6-(3-((4S,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)prop-1-enyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethoxy)(tert-butyl)diphenylsilane

Guidance literature:: 5-(2-((4R,6S)-6-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxan-4-yl)ethylsulfonyl)-1-phenyl-1H-tetrazole; (4S,6S)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)-2,2-dimethyl-1,3-dioxane-4-carbaldehyde; With lithium hexamethyldisilazane; In 1,2-dimethoxyethane; hexane; at -78 ℃; for 20h;

With 18-crown-6 ether; lithium hexamethyldisilazane; In 1,2-dimethoxyethane; hexane; at 20 ℃; for 18h; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2008.07.022