4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

Base Information

Chemical Name:4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene
CAS No.:1360569-03-4
Molecular Formula:C₂₁H₂₂BrClF₂O
Molecular Weight:443.759
Hs Code.:

Synonyms:4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

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Chemical Property of 4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

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Technology Process of 4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

There total 11 articles about 4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.9%

: 864070-18-8
4-(5-bromo-2-chlorobenzyl)phenol

: 1360568-92-8
(4,4-difluoro-1-methylcyclohexyl)methyl 4-methylbenzenesulfonate

: 1360569-03-4
4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 5h; Inert atmosphere;

Reference yield:

: 461432-22-4
(5-bromo-2-chlorophenyl)(4-ethyloxyphenyl)methanone

: 1360569-03-4
4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

2: triethylsilane; boron trifluoride diethyl etherate / diethyl ether; dichloromethane; acetonitrile / 16 h / 20 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere

With triethylsilane; boron trifluoride diethyl etherate; aluminum (III) chloride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 1360569-03-4
4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

2: aluminum (III) chloride / dichloromethane / 1 h / 0 °C

3: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

4: triethylsilane; boron trifluoride diethyl etherate / diethyl ether; dichloromethane; acetonitrile / 16 h / 20 °C / Inert atmosphere

5: N,N-dimethyl-formamide / 5 h / 120 °C / Inert atmosphere

With triethylsilane; thionyl chloride; boron trifluoride diethyl etherate; aluminum (III) chloride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;