4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside
CAS No.:866325-75-9
Molecular Formula:C₆₃H₅₄O₁₇
Molecular Weight:1083.11
Hs Code.:

Synonyms:4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Suppliers and Price of 4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

There total 7 articles about 4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 866325-72-6
allyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

: 5720-07-0
4-methoxyphenylboronic acid

: 866325-75-9
4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Guidance literature:: With lithium acetate; copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 1h;
DOI:10.1016/j.tetasy.2005.06.040

Reference yield:

: 866325-71-5
allyl 6-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

: 866325-75-9
4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dimethylformamide / 18 h / 20 °C

2: 0.52 g / aq. HCl / tetrahydrofuran / 12 h / 20 °C

3: 85 percent / tetramethylurea; AgOTf / CH₂Cl₂ / 12 h / 20 °C

4: 25 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 1 h / 100 °C

With pyridine; hydrogenchloride; lithium acetate; copper diacetate; silver trifluoromethanesulfonate; palladium diacetate; tetramethylurea; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2005.06.040

Reference yield:

: 866325-70-4
allyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: 866325-75-9
4-methoxycinnamyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-L-arabinopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetramethylurea; AgOTf / CH₂Cl₂ / 12 h / 20 °C

2: 25 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 1 h / 100 °C

With lithium acetate; copper diacetate; silver trifluoromethanesulfonate; palladium diacetate; tetramethylurea; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2005.06.040