methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside

Base Information

Chemical Name:methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside
CAS No.:128657-65-8
Molecular Formula:C₁₈H₂₃NO₇
Molecular Weight:365.383
Hs Code.:

Synonyms:methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside

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Technology Process of methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside

There total 11 articles about methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 108-24-7
acetic anhydride

: 6082-04-8
methyl 2-acetylamido-2-deoxy-D-glucoside

: 6748-94-3,35439-46-4,52885-38-8,78216-84-9,98574-00-6,99944-67-9,109121-60-0,109121-61-1,110658-08-7,128657-65-8,129784-18-5,139894-30-7,87303-57-9
methyl 2-acetamido-3-O-acetyl-4,6-di-O-benzylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: benzaldehyde dimethyl acetal; methyl 2-acetylamido-2-deoxy-D-glucoside; With toluene-4-sulfonic acid; In acetonitrile; at 25 ℃; Inert atmosphere;

acetic anhydride; In acetonitrile; at 40 ℃; Inert atmosphere;
DOI:10.1055/s-0028-1087913

Reference yield:

: 116561-28-5
methyl 2-amino-2-deoxy-4,6-O-(phenylmethylene)-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 128657-65-8
methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1080/07328303.2018.1524012

Reference yield:

: 2880-96-8,3150-15-0,3150-16-1,3257-59-8,14187-71-4,15384-57-3,19465-13-5,32976-15-1,52885-37-7,53270-02-3,53270-03-4,65391-11-9,65391-12-0,66537-92-6,67226-04-4,71184-14-0,86420-78-2,86420-79-3,91177-51-4,91177-52-5,117708-93-7,120408-72-2
methyl 2,3-anhydro-4,6-dioxabenzylidene-α-D-gulopyranose

: 6748-94-3,35439-46-4,52885-38-8,78216-84-9,87303-57-9,98574-00-6,99944-67-9,109121-60-0,109121-61-1,110658-08-7,128657-65-8,129784-18-5,139894-30-7
methyl-[O³-acetyl-2-acetylamino-O⁴,O⁶-((S)-benzylidene)-2-deoxy-α-D-idopyranoside]

Guidance literature:: With ammonium hydroxide; at 120 ℃; Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin;
DOI:10.1021/ja01241a003 DOI:10.1039/jr9600003392