phenylcarbamatobis(triphenylphosphine)copper(I)

Base Information

• Chemical Name: phenylcarbamatobis(triphenylphosphine)copper(I)
• CAS No.: 73716-94-6
• Molecular Formula: C₄₃H₃₆CuNO₂P₂
• Molecular Weight: 724.258
• Mol file: 73716-94-6.mol

Synonyms:phenylcarbamatobis(triphenylphosphine)copper(I)

Chemical Property of phenylcarbamatobis(triphenylphosphine)copper(I)

Chemical Property:

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Technology Process of phenylcarbamatobis(triphenylphosphine)copper(I)

There total 1 articles about phenylcarbamatobis(triphenylphosphine)copper(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

hydrogencarbonatobis(triphenylphosphine)copper(I) (73716-93-5) → phenylcarbamatobis(triphenylphosphine)copper(I) (73716-94-6)

Guidance literature:

With aniline; In N,N-dimethyl-formamide; under N2, Cu complex dissolved in DMF containing aniline, mixt. stirredat -30°C under CO2 for 10 h; added diethyl ether and hexane, cooled to -78°C, filtered, driedin vac., elem. anal.;

DOI:10.1246/bcsj.53.680

upstream raw materials:

hydrogencarbonatobis(triphenylphosphine)copper(I)