C₂₆H₂₈N₂O₂

Base Information

Chemical Name:C₂₆H₂₈N₂O₂
CAS No.:1572572-05-4
Molecular Formula:C₂₆H₂₈N₂O₂
Molecular Weight:400.521
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₆H₂₈N₂O₂

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Chemical Property of C₂₆H₂₈N₂O₂

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Technology Process of C₂₆H₂₈N₂O₂

There total 9 articles about C₂₆H₂₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1572572-02-1
C₂₆H₂₈N₂O₃

: 1572572-05-4
C₂₆H₂₈N₂O₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -20 ℃; for 5h; enantioselective reaction;
DOI:10.1021/jo402741g

Reference yield:

: 73825-32-8
3-(2-Methoxy-phenylamino)-cyclohex-2-enone

: 1572572-05-4
C₂₆H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

2.2: 2 h / 0 - 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C

4.2: 0.05 h / 0 °C

5.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / toluene / 12 h / 20 - 70 °C / Inert atmosphere

6.1: formic acid / 20 °C

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / -20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; formic acid; potassium tert-butylate; copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo402741g

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 1572572-05-4
C₂₆H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene-4-sulfonic acid / toluene

2.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

3.2: 2 h / 0 - 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C

5.2: 0.05 h / 0 °C

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / toluene / 12 h / 20 - 70 °C / Inert atmosphere

7.1: formic acid / 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / -20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; formic acid; potassium tert-butylate; copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo402741g