2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester

Base Information

• Chemical Name: 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester
• CAS No.: 526209-36-9
• Molecular Formula: C₂₇H₃₂N₂Te
• Molecular Weight: 512.164
• Mol file: 526209-36-9.mol

Synonyms:2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester

Chemical Property of 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester

There total 1 articles about 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) + N-(2,2-dimethylpropylidene)benzylamine (1775-74-2) + triethoxysilyl phenyl telluride (526209-50-7) → 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester (526209-36-9)

Guidance literature:

In acetonitrile; at 25 ℃; for 24h;

DOI:10.1002/anie.200390039

Reference yield: 94.0%

mercury(II) diacetate (1600-27-7) + 2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester (526209-36-9) → 2-(acetyl-benzyl-amino)-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-butyramide

Guidance literature:

With benzenesulfonamide; water; In tetrahydrofuran; at 20 ℃; for 0.25h;

DOI:10.1002/anie.200390039

Reference yield: 76.0%

2-benzylamino-N-(2,6-dimethyl-phenyl)-3,3-dimethyl-tellurobutyrimidic acid phenyl ester (526209-36-9) → [2-Benzylamino-3,3-dimethyl-but-(E)-ylidene]-(2,6-dimethyl-phenyl)-amine (526209-47-2)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at -72 ℃; for 0.2h;

DOI:10.1002/anie.200390039

upstream raw materials:

2,6-dimethylphenyl isonitrile

N-(2,2-dimethylpropylidene)benzylamine

triethoxysilyl phenyl telluride

Downstream raw materials:

[2-Benzylamino-3,3-dimethyl-but-(E)-ylidene]-(2,6-dimethyl-phenyl)-amine