C₃₄H₃₄F₂N₂O₅

Base Information

Chemical Name:C₃₄H₃₄F₂N₂O₅
CAS No.:950599-94-7
Molecular Formula:C₃₄H₃₄F₂N₂O₅
Molecular Weight:588.651
Hs Code.:

C<sub>34</sub>H<sub>34</sub>F<sub>2</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₄H₃₄F₂N₂O₅

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Chemical Property of C₃₄H₃₄F₂N₂O₅

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Technology Process of C₃₄H₃₄F₂N₂O₅

There total 14 articles about C₃₄H₃₄F₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 950599-47-0
C₃₄H₃₂F₂N₂O₅

: 950599-94-7
C₃₄H₃₄F₂N₂O₅

Guidance literature:: With sodium tetrahydroborate; diethyl methoxy borane; acetic acid; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/j.tet.2007.06.005 DOI:10.1016/j.bmcl.2007.05.096

Reference yield:

: C₁₄H₉F₂NO₂

: 950599-94-7
C₃₄H₃₄F₂N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1: 38 percent / DBU / tetrahydrofuran / 12 h / 25 °C

2: 62 percent / KOH / dimethylsulfoxide / 1.5 h / 25 °C

3: 45 percent / POCl₃ / 1,2-dichloro-ethane / 3 h / 80 °C

4: 100 percent / NaOH / methanol / 2 h / 60 °C

5: SOCl₂ / 80 °C

6: Et₃N / tetrahydrofuran / 12 h / 25 °C

7: 66 percent / toluene / 48 h / 110 °C

8: 99 percent / aq. HF / acetonitrile / 2 h / 0 °C

9: 58 percent / Et₂B(OMe); NaBH₄; AcOH / tetrahydrofuran / 2 h / -78 °C

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; diethyl methoxy borane; hydrogen fluoride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene; acetonitrile; 1: Barton-Zard reaction / 3: Vilsmeir-Haack reaction / 7: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096

Reference yield:

: 855248-37-2
3,4-bis-(4-fluorophenyl)-5-formyl-1-isopropyl-1H-pyrrole-2-carboxylic acid ethyl ester

: 950599-94-7
C₃₄H₃₄F₂N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / NaOH / methanol / 2 h / 60 °C

2: SOCl₂ / 80 °C

3: Et₃N / tetrahydrofuran / 12 h / 25 °C

4: 66 percent / toluene / 48 h / 110 °C

5: 99 percent / aq. HF / acetonitrile / 2 h / 0 °C

6: 58 percent / Et₂B(OMe); NaBH₄; AcOH / tetrahydrofuran / 2 h / -78 °C

With sodium hydroxide; sodium tetrahydroborate; thionyl chloride; diethyl methoxy borane; hydrogen fluoride; acetic acid; triethylamine; In tetrahydrofuran; methanol; toluene; acetonitrile; 4: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096