(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Base Information

Chemical Name:(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl
CAS No.:74444-94-3
Molecular Formula:C₄₀H₄₁NO₅*ClH
Molecular Weight:652.23
Hs Code.:

Synonyms:(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Suppliers and Price of (+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

There total 3 articles about (+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 74444-93-2
2-Benzyl-1-(3,4,5-trimethoxybenzoyl)-6,7-dibenzyloxy-3,4-dihydroxy-isochinoliniumbromid

: 74444-94-3
(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: With propionic acid; zinc; for 2h; Heating;

Reference yield:

: 55536-68-0
1-(3,4,5-Trimethoxybenzoyl)-6,7-dibenzyloxy-3,4-dihydroisochinolin

: 74444-94-3
(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / dimethylformamide / 1 h / 100 °C

2: 49 percent / propionic acid, Zn / 2 h / Heating

With propionic acid; zinc; In N,N-dimethyl-formamide;

Reference yield:

: 37481-62-2
N-<3,4-bis(benzyloxy)phenylethyl>-3,4,5-trimethoxyphenylacetamide

: 74444-94-3
(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.)POCl₃ 2.)O₂ / 1.)Acetonitril, 120 min., reflux. 2.)Benzene 60 deg C, 90 min.

2: 88 percent / dimethylformamide / 1 h / 100 °C

3: 49 percent / propionic acid, Zn / 2 h / Heating

With oxygen; propionic acid; zinc; trichlorophosphate; In N,N-dimethyl-formamide;