(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Base Information

Chemical Name:(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl
CAS No.:74444-95-4
Molecular Formula:C₁₉H₂₃NO₅*ClH
Molecular Weight:381.856
Hs Code.:

Synonyms:(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

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Chemical Property of (+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

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Technology Process of (+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

There total 4 articles about (+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 74444-94-3
(+/-) 3-Benzyl-2-(3,4,5-trimethoxyphenyl)-7,8-dibenzyloxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

: 74444-95-4
(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1h; under 760 Torr; Ambient temperature;

Reference yield:

: 55536-68-0
1-(3,4,5-Trimethoxybenzoyl)-6,7-dibenzyloxy-3,4-dihydroisochinolin

: 74444-95-4
(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / dimethylformamide / 1 h / 100 °C

2: 49 percent / propionic acid, Zn / 2 h / Heating

3: 68 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr / Ambient temperature

With hydrogen; propionic acid; zinc; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 37481-62-2
N-<3,4-bis(benzyloxy)phenylethyl>-3,4,5-trimethoxyphenylacetamide

: 74444-95-4
(+/-) 2-(3,4,5-Trimethoxyphenyl)-7,8-dihydroxy-2,3,4,5-tetrahydro-1H-3-benzazepin. HCl

Guidance literature:: Multi-step reaction with 4 steps

1: 1.)POCl₃ 2.)O₂ / 1.)Acetonitril, 120 min., reflux. 2.)Benzene 60 deg C, 90 min.

2: 88 percent / dimethylformamide / 1 h / 100 °C

3: 49 percent / propionic acid, Zn / 2 h / Heating

4: 68 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr / Ambient temperature

With hydrogen; oxygen; propionic acid; zinc; trichlorophosphate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;