(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

Base Information

Chemical Name:(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite
CAS No.:462102-47-2
Molecular Formula:C₂₇H₃₄NO₃P
Molecular Weight:451.546
Hs Code.:

Synonyms:(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

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Chemical Property of (1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

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Technology Process of (1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

There total 1 articles about (1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 552-79-4
(-)-N-methylephedrine

: 22277-52-7
di(2,6-dimethoxyphenyl) chlorophosphite

: 462102-47-2
(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

Guidance literature:: With triethylamine; In benzene; at 50 ℃; for 1h;
DOI:10.1002/1099-0682(200206)2002:6<1367::aid-ejic1367>3.0.co;2-f

Reference yield: 87.0%

: di(rhodium)tetracarbonyl dichloride

: 462102-47-2
(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite

: [(1R,2S)-2-dimethylamino-1-phenylpropyl bis(2,6-dimethylphenyl)phosphite]Rh(CO)Cl

Guidance literature:: In chloroform; byproducts: CO; under Ar, 2 equiv. of phosphite-compd. in CHCl3 was dropwise added a stirred soln. of Rh-compd in CHCl3 at 20 °C, stirring for 30 min at this temp.; solvent was removed in vac. (40 Torr), hexane was added, ppt. was centrifuged off, washed twice with hexane, dried in vac. (2 Torr), elem. anal.;
DOI:10.1002/1099-0682(200206)2002:6<1367::aid-ejic1367>3.0.co;2-f