C₂₇H₂₉N₃O₆S

Base Information

Chemical Name:C₂₇H₂₉N₃O₆S
CAS No.:1333120-84-5
Molecular Formula:C₂₇H₂₉N₃O₆S
Molecular Weight:523.61
Hs Code.:

C<sub>27</sub>H<sub>29</sub>N<sub>3</sub>O<sub>6</sub>S

Synonyms:C₂₇H₂₉N₃O₆S

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Chemical Property of C₂₇H₂₉N₃O₆S

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Technology Process of C₂₇H₂₉N₃O₆S

There total 7 articles about C₂₇H₂₉N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1333120-83-4
C₃₆H₄₇N₃O₉S

: 1333120-84-5
C₂₇H₂₉N₃O₆S

Guidance literature:: C₃₆H₄₇N₃O₉S; With methanol; thionyl chloride; at 0 - 20 ℃; for 2h; Inert atmosphere;

With trichlorophosphate; In toluene; at 120 ℃; Inert atmosphere;

With trifluoroacetic acid; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol2020362

Reference yield:

: 1333120-91-4
C₁₄H₂₇NO₄

: 1333120-84-5
C₂₇H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate; rhodium(III) chloride hydrate / water; acetonitrile / 16 h / 20 °C / Inert atmosphere

2.1: diisopropyl-carbodiimide / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

3.3: -78 - 20 °C / Inert atmosphere

4.1: methanol; thionyl chloride / 2 h / 0 - 20 °C / Inert atmosphere

4.2: 120 °C / Inert atmosphere

4.3: 48 h / 20 °C / Inert atmosphere

With methanol; sodium periodate; thionyl chloride; rhodium(III) chloride hydrate; lithium hexamethyldisilazane; diisopropyl-carbodiimide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; water; acetonitrile;
DOI:10.1021/ol2020362

Reference yield:

: 191013-97-5
tert-butyl (2R)-(-)-methylpiperidine-1-carboxylate

: 1333120-84-5
C₂₇H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether; cyclohexane / 7 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

1.3: -78 - 20 °C / Inert atmosphere

2.1: 1,4-diaza-bicyclo[2.2.2]octane; osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 20 °C / Inert atmosphere

3.1: sodium periodate; rhodium(III) chloride hydrate / water; acetonitrile / 16 h / 20 °C / Inert atmosphere

4.1: diisopropyl-carbodiimide / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

5.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / -78 °C / Inert atmosphere

5.2: -78 °C / Inert atmosphere

5.3: -78 - 20 °C / Inert atmosphere

6.1: methanol; thionyl chloride / 2 h / 0 - 20 °C / Inert atmosphere

6.2: 120 °C / Inert atmosphere

6.3: 48 h / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; methanol; sodium periodate; osmium(VIII) oxide; thionyl chloride; N,N,N,N,-tetramethylethylenediamine; rhodium(III) chloride hydrate; sec.-butyllithium; potassium carbonate; lithium hexamethyldisilazane; potassium hexacyanoferrate(III); diisopropyl-carbodiimide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; cyclohexane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol2020362