17β--4-methyl-4-aza-5α-androstan-3-one

Base Information

• Chemical Name: 17β--4-methyl-4-aza-5α-androstan-3-one
• CAS No.: 162893-43-8
• Molecular Formula: C₂₆H₃₈N₂O₂
• Molecular Weight: 410.6

Synonyms:17β--4-methyl-4-aza-5α-androstan-3-one

Chemical Property of 17β--4-methyl-4-aza-5α-androstan-3-one

Chemical Property:

Purity/Quality:

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Technology Process of 17β--4-methyl-4-aza-5α-androstan-3-one

There total 1 articles about 17β--4-methyl-4-aza-5α-androstan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4aR,4bS,6aS,9aS,9bR,11aR)-7-[(E)-4-Methoxy-phenylimino]-1,4a,6a-trimethyl-hexadecahydro-indeno[5,4-f]quinolin-2-one → 17β--4-methyl-4-aza-5α-androstan-3-one (162893-43-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 1h; Yield given; Ambient temperature;

DOI:10.1021/jm00007a013

Reference yield: 99.0%

isobutyryl chloride (79-30-1) + 17β--4-methyl-4-aza-5α-androstan-3-one (162893-43-8) → 17β--4-methyl-4-aza-5α-androstan-3-one

Guidance literature:

for 16h; Heating;

DOI:10.1021/jm00007a013

Reference yield: 94.0%

benzoyl chloride (98-88-4) + 17β--4-methyl-4-aza-5α-androstan-3-one (162893-43-8) → 17β--4-methyl-4-aza-5α-androstan-3-one

Guidance literature:

With potassium carbonate; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jm00007a013

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