phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Base Information

Chemical Name:phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate
CAS No.:118493-90-6
Molecular Formula:C₂₄H₂₉NO₉
Molecular Weight:475.496
Hs Code.:

Synonyms:phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Suppliers and Price of phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

There total 5 articles about phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-24-7
acetic anhydride

: 118493-89-3
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

: 118493-90-6
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Guidance literature:: With pyridine;
DOI:10.1016/0040-4039(88)85118-9 DOI:10.1021/jo00267a017

Reference yield:

: 19479-65-3
2-ethoxyacrylonitrile

: 118493-90-6
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / aq. ethanol / 74 h / Irradiation

2: 93 percent / pyridine

With pyridine; In ethanol;
DOI:10.1021/jo00267a017

Reference yield:

: 15548-45-5
(2S,3S,4S,5S,6R)-2-benzyloxy-6-(hydroxymethyl)tetrahydropyran-3,4,5-triol

: 118493-90-6
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile 2,3,4-tri-O-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: NaI, CH₃CN

3: 1.) NaCo(dmgH)2py / 1.) MeOH,H₂O, 2.) visible light, 95percent EtOH, 48 h.

4: 93 percent / pyridine

With pyridine; Na; acetonitrile; sodium iodide;
DOI:10.1016/0040-4039(88)85118-9