phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

Base Information

Chemical Name:phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile
CAS No.:118493-89-3
Molecular Formula:C₁₈H₂₃NO₆
Molecular Weight:349.384
Hs Code.:

Synonyms:phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

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Chemical Property of phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

Chemical Property:

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Technology Process of phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

There total 3 articles about phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 19479-65-3
2-ethoxyacrylonitrile

: 118493-89-3
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

Guidance literature:: In ethanol; for 74h; Irradiation;
DOI:10.1021/jo00267a017

Reference yield:

: 117371-06-9
benzyl 6-O-p-toluenesulfonyl-α-D-mannopyranoside

: 118493-89-3
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: NaI, CH₃CN

2: 1.) NaCo(dmgH)2py / 1.) MeOH,H₂O, 2.) visible light, 95percent EtOH, 48 h.

With Na; acetonitrile; sodium iodide;
DOI:10.1016/0040-4039(88)85118-9

Reference yield:

: 19479-65-3
2-ethoxyacrylonitrile

: 117370-99-7
phenylmethyl 6-deoxy-6-iodo-α-D-mannopyranoside

: 118493-89-3
phenylmethyl 6,7-dideoxy-8-O-ethyl-α-D-manno-non-7-enopyranosidurononitrile

Guidance literature:: With Na; Yield given. Multistep reaction; 1.) MeOH,H₂O, 2.) visible light, 95percent EtOH, 48 h.;
DOI:10.1016/0040-4039(88)85118-9