C₄₀H₅₄ClNO₅

Base Information

Chemical Name:C₄₀H₅₄ClNO₅
CAS No.:1449797-08-3
Molecular Formula:C₄₀H₅₄ClNO₅
Molecular Weight:664.325
Hs Code.:

C<sub>40</sub>H<sub>54</sub>ClNO<sub>5</sub>

Synonyms:C₄₀H₅₄ClNO₅

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Chemical Property of C₄₀H₅₄ClNO₅

Chemical Property:

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Technology Process of C₄₀H₅₄ClNO₅

There total 7 articles about C₄₀H₅₄ClNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 5467-71-0
4-chlorophenacylamine hydrochloride

: 374901-99-2
(3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-acetoxy-1-iso propyl-5a,5b,8,8,8,11a-pentamethyl-2-oxo-2,3,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-3aH-cyclopenta[a]chrysene-3a-carboxylic acid

: 1449797-08-3
C₄₀H₅₄ClNO₅

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 473-98-3
betulin

: 1449797-08-3
C₄₀H₅₄ClNO₅

Guidance literature:: Multi-step reaction with 7 steps

1: toluene / 3 h / 100 °C

2: acetic anhydride; hydrogen bromide; acetic acid / toluene / 1.5 h / 105 °C

3: acetic anhydride; acetic acid; sodium acetate; sodium dichromate / toluene / 60 °C

4: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

5: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C

6: methylbutane; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1 h / 20 °C

7: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; sodium dichromate; methylbutane; hydrogen bromide; sodium acetate; acetic anhydride; silica gel; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; potassium hydroxide; In ethanol; dichloromethane; water; toluene; tert-butyl alcohol;

Reference yield:

: 1721-69-3
betulin diacetate

: 1449797-08-3
C₄₀H₅₄ClNO₅

Guidance literature:: Multi-step reaction with 6 steps

1: acetic anhydride; hydrogen bromide; acetic acid / toluene / 1.5 h / 105 °C

2: acetic anhydride; acetic acid; sodium acetate; sodium dichromate / toluene / 60 °C

3: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

4: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C

5: methylbutane; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1 h / 20 °C

6: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; sodium dichromate; methylbutane; hydrogen bromide; sodium acetate; acetic anhydride; silica gel; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; potassium hydroxide; In ethanol; dichloromethane; water; toluene; tert-butyl alcohol;