1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

Base Information

Chemical Name:1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate
CAS No.:1402073-75-9
Molecular Formula:C₃₃H₃₀N₄O₄
Molecular Weight:546.626
Hs Code.:

Synonyms:1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

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Chemical Property of 1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

Chemical Property:

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Technology Process of 1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

There total 6 articles about 1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1424832-40-5
1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propanol

: 530-62-1
1,1'-carbonyldiimidazole

: 1402073-75-9
1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

Guidance literature:: In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1402073-75-9
1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium tetrachloride / dichloromethane / 0.5 h / -78 °C

2.1: ozone / methanol / 0.08 h / -78 °C

2.2: 0.5 h / -78 - 20 °C

3.1: triethylamine; dmap / dichloromethane / 20 °C / Cooling with ice

4.1: tetrahydrofuran / 72 h / 20 °C

5.1: triethylamine / acetonitrile / 0.5 h / 20 °C

6.1: dichloromethane / 4 h / 20 °C

With dmap; titanium tetrachloride; ozone; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;

Reference yield:

: 125715-24-4
1-(2-nitrophenyl)but-3-en-1-ol

: 1402073-75-9
1-(2-nitrophenyl)-3-(N-methyl-N-tritylamino)propyl 1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: ozone / methanol / 0.08 h / -78 °C

1.2: 0.5 h / -78 - 20 °C

2.1: triethylamine; dmap / dichloromethane / 20 °C / Cooling with ice

3.1: tetrahydrofuran / 72 h / 20 °C

4.1: triethylamine / acetonitrile / 0.5 h / 20 °C

5.1: dichloromethane / 4 h / 20 °C

With dmap; ozone; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;