(1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

Base Information

Chemical Name:(1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene
CAS No.:1071850-40-2
Molecular Formula:C₃₈H₆₆O₅Si₂
Molecular Weight:659.11
Hs Code.:

Synonyms:(1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

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Chemical Property of (1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

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Technology Process of (1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

There total 1 articles about (1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1071850-38-8
(1R,2R,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-6-(triisopropylsiloxy)hex-4-en-3-ol

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1071850-40-2
(1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 23h; Inert atmosphere;
DOI:10.1002/anie.200802079

Reference yield:

: 1071850-40-2
(1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene

: C₃₈H₆₆O₆Si₂

Guidance literature:: (1R,2S,3R,Z)-1-(furan-2-yl)-1-(4-methoxybenzyloxy)-2,4-dimethyl-3,6-bis(triisopropylsiloxy)hex-4-ene; With oxygen; rose bengal; In propiononitrile; at -78 ℃; for 8h; Irradiation;

With dimethylsulfide; In propiononitrile; at -78 - -20 ℃; for 15h; Inert atmosphere;
DOI:10.1002/anie.200802079