C₄₁H₄₃F₉O₈SSi

Base Information

Chemical Name:C₄₁H₄₃F₉O₈SSi
CAS No.:303998-29-0
Molecular Formula:C₄₁H₄₃F₉O₈SSi
Molecular Weight:894.925
Hs Code.:

C<sub>41</sub>H<sub>43</sub>F<sub>9</sub>O<sub>8</sub>SSi

Synonyms:C₄₁H₄₃F₉O₈SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₃F₉O₈SSi

Chemical Property:

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Technology Process of C₄₁H₄₃F₉O₈SSi

There total 11 articles about C₄₁H₄₃F₉O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: C₃₇H₄₄O₆Si

: 303998-29-0
C₄₁H₄₃F₉O₈SSi

Guidance literature:: With triethylamine; In dichloromethane; at 23 ℃; for 18h;
DOI:10.1021/ja0024892

Reference yield:

: (2R,4bR)-8-Allyloxy-2-(dimethyl-phenyl-silanyl)-4a-methyl-11-triethylsilanyloxy-2,3,4a,4b,5,6,12,12a-octahydro-1H-chrysen-4-one

: 303998-29-0
C₄₁H₄₃F₉O₈SSi

Guidance literature:: Multi-step reaction with 10 steps

1: 90 percent / LiAlH₄ / diethyl ether / 0.5 h / -78 °C

2: 92 percent / i-Pr₂NEt / CH₂Cl₂ / 46 h / 23 °C

3: 89 percent / p-TsOH / CH₂Cl₂; methanol / 0.08 h / 23 °C

4: LDA / tetrahydrofuran / 0.33 h / -78 °C

5: 856 mg / O₂; Pd(OAc)2; 2,6-di-tert-butyl-4-methylpyridine / dimethylsulfoxide / 12 h / 25 °C

6: L-selectride / tetrahydrofuran / 0.33 h / -78 °C

7: 564 mg / t-BuOOH; VO(acac)2 / CH₂Cl₂; decane / 20 h / 0 °C

8: 97 percent / Et₃N; DMAP / CH₂Cl₂ / 3 h / 25 °C

9: Pd(Ph₃P)4; Et₂NH / CH₂Cl₂ / 3 h / Heating

10: 690 mg / Et₃N / CH₂Cl₂ / 18 h / 23 °C

With tert.-butylhydroperoxide; dmap; palladium diacetate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; bis(acetylacetonate)oxovanadium; oxygen; L-Selectride; toluene-4-sulfonic acid; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; decane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja0024892

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 303998-29-0
C₄₁H₄₃F₉O₈SSi

Guidance literature:: Multi-step reaction with 9 steps

1: 92 percent / i-Pr₂NEt / CH₂Cl₂ / 46 h / 23 °C

2: 89 percent / p-TsOH / CH₂Cl₂; methanol / 0.08 h / 23 °C

3: LDA / tetrahydrofuran / 0.33 h / -78 °C

4: 856 mg / O₂; Pd(OAc)2; 2,6-di-tert-butyl-4-methylpyridine / dimethylsulfoxide / 12 h / 25 °C

5: L-selectride / tetrahydrofuran / 0.33 h / -78 °C

6: 564 mg / t-BuOOH; VO(acac)2 / CH₂Cl₂; decane / 20 h / 0 °C

7: 97 percent / Et₃N; DMAP / CH₂Cl₂ / 3 h / 25 °C

8: Pd(Ph₃P)4; Et₂NH / CH₂Cl₂ / 3 h / Heating

9: 690 mg / Et₃N / CH₂Cl₂ / 18 h / 23 °C

With tert.-butylhydroperoxide; dmap; palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; bis(acetylacetonate)oxovanadium; oxygen; L-Selectride; toluene-4-sulfonic acid; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; decane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja0024892