(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

Base Information

Chemical Name:(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester
CAS No.:210985-57-2
Molecular Formula:C₂₆H₂₈N₂O₈
Molecular Weight:496.517
Hs Code.:

Synonyms:(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

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Technology Process of (2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

There total 2 articles about (2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.3%

: 638-37-9
butanedial

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: (2E,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

: 210985-57-2
(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; Yields of byproduct given; 1) 5-10 deg C, 1 h, 2.) room temp., overnight;
DOI:10.1021/jo982034j

Reference yield:

: 638-37-9
butanedial

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: (2Z)-2-(benzyloxycarbonylamino)-1-carboxyhex-2-en-6-al methyl ester hydrate

: (2E,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

: 210985-57-2
(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

Guidance literature:: With 1,1,3,3-tetramethylguanidine;
DOI:10.1021/jo982034j

Reference yield: 85.0%

: 210985-57-2
(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

: 73872-72-7
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

: (2S,7R)-2,7-Bis-benzyloxycarbonylamino-octanedioic acid dimethyl ester

Guidance literature:: With (+)-1,2-bis-((2S,5S)-2,5-diethylphospholano)benzene(cyclooctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; In methanol; for 18h; under 3000.24 Torr; Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo982034j