ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

Base Information

Chemical Name:ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate
CAS No.:1356353-68-8
Molecular Formula:C₁₇H₂₂N₂O₅
Molecular Weight:334.372
Hs Code.:

Synonyms:ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

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Chemical Property of ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

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Technology Process of ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

There total 3 articles about ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356353-65-5
ethyl 4-[(2,4-dimethoxybenzyl)amino]butanoate

: 16712-16-6,64165-14-6,65387-22-6,70179-79-2,540-69-2
ammonium formate

: 1356353-68-8
ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

Guidance literature:: ethyl 4-[(2,4-dimethoxybenzyl)amino]butanoate; With monomethyl oxalyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.25h;

With ethanol; sodium ethanolate; for 0.5h; Reflux;

ammonium formate; Further stages;

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 1356353-68-8
ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 1 h / Reflux

1.2: 1 h / 20 °C

2.1: triethylamine; monomethyl oxalyl chloride / tetrahydrofuran / 0.25 h / 20 °C

2.2: 0.5 h / Reflux

With monomethyl oxalyl chloride; triethylamine; In tetrahydrofuran; ethanol;

Reference yield:

: 6937-16-2
ethyl γ-aminobutyrate hydrochloride

: 1356353-68-8
ethyl 5-amino-1-(2,4-dimethoxybenzyl)-6-oxo-1,2,3,6-tetrahydropyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 1 h / Reflux

1.2: 1 h / 20 °C

2.1: triethylamine; monomethyl oxalyl chloride / tetrahydrofuran / 0.25 h / 20 °C

2.2: 0.5 h / Reflux

With monomethyl oxalyl chloride; triethylamine; In tetrahydrofuran; ethanol;