octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

Base Information

Chemical Name:octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside
CAS No.:685111-76-6
Molecular Formula:C₄₆H₄₉N₃O₁₂
Molecular Weight:835.908
Hs Code.:

Synonyms:octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

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Chemical Property of octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

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Technology Process of octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

There total 4 articles about octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 569659-32-1
octyl 2,5-di-O-benzoyl-α-D-arabinofuranoside

: 685111-65-3
p-toluyl 5-azido-2,3-di-O-benzoyl-5-deoxy-1-thio-α-D-arabinofuranoside

: 685111-76-6
octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.0833333h;
DOI:10.1016/j.carres.2003.12.015

Reference yield:

: 98-88-4
benzoyl chloride

: 685111-76-6
octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine / 12 h / 20 °C

2: 91 percent / sodium azide; 18-crown-6 / dimethylformamide / 50 °C

3: 84 percent / N-iodosuccinimide; silver triflate / CH₂Cl₂ / 0.08 h / 0 °C

With pyridine; N-iodo-succinimide; sodium azide; 18-crown-6 ether; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2003.12.015

Reference yield:

: 204918-49-0
p-methylphenyl 1-thio-α-D-arabinofuranoside

: 685111-76-6
octyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-arabinofuranosyl-(1->3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / DMAP; pyridine / CH₂Cl₂ / 20 °C

2: 84 percent / pyridine / 12 h / 20 °C

3: 91 percent / sodium azide; 18-crown-6 / dimethylformamide / 50 °C

4: 84 percent / N-iodosuccinimide; silver triflate / CH₂Cl₂ / 0.08 h / 0 °C

With pyridine; dmap; N-iodo-succinimide; sodium azide; 18-crown-6 ether; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2003.12.015