6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

Base Information

Chemical Name:6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate
CAS No.:1259401-73-4
Molecular Formula:C₂₅H₂₀N₂O₅S
Molecular Weight:460.51
Hs Code.:

Synonyms:6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

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Technology Process of 6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

There total 1 articles about 6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 937187-84-3
1,2-HOPO-2

: 98-09-9
benzenesulfonyl chloride

: 1259401-73-4
6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

Guidance literature:: With pyridine; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1007/s00775-010-0727-x

Reference yield:

: 1259401-73-4
6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

: 937187-84-3
1,2-HOPO-2

Guidance literature:: With dihydrogen peroxide;
DOI:10.1007/s00775-010-0727-x

Reference yield:

: 1259401-73-4
6-((1,1'-biphenyl-4-ylmethyl)carbamoyl)-2-oxopyridin-1(2H)-yl benzenesulfonate

: 1223525-51-6
N-(biphenyl-4-ylmethyl)-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-1,6-dihydropyridin-6(1H)-one-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / 20 °C / pH 7.5 / HEPES buffer

2: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With dihydrogen peroxide; caesium carbonate; In N,N-dimethyl-formamide;