3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

Base Information

Chemical Name:3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose
CAS No.:213776-93-3
Molecular Formula:C₄₁H₄₆O₆
Molecular Weight:634.813
Hs Code.:

Synonyms:3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

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Chemical Property of 3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

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Technology Process of 3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

There total 2 articles about 3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 627-27-0
homoalylic alcohol

: 776313-98-5
5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy-D-gluco-non-1-eno-4-ulopyranose

: 213776-93-3
3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

Guidance literature:: With 4 A molecular sieve; montmorillonite K-10; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(98)01247-7

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 213776-93-3
3-buten-1-yl (5,6,7,9-tetra-O-benzyl-1,2,3-trideoxy)-α-D-gluco-non-1-eno-4-ulopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / diethyl ether / -78 °C

2: 69 percent / Montmorillonite K-10 clay; 4 Angstroem molecualr sieves / CH₂Cl₂ / 20 °C

With 4 A molecular sieve; Montmorillonite K-10 clay; In diethyl ether; dichloromethane;
DOI:10.1039/b401699h