5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Base Information

Chemical Name:5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate
CAS No.:123549-80-4
Molecular Formula:C₇H₇O₃S*C₂₄H₂₀ClINO
Molecular Weight:671.983
Hs Code.:

Synonyms:5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

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Chemical Property of 5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

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Technology Process of 5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

There total 3 articles about 5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 123466-28-4
[(4-chlorophenyl)ethynyl](phenyl)iodonium tosylate

: 2904-57-6
mesitylenecarbonitrile oxide

: 123549-80-4
5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Guidance literature:: In dichloromethane; for 48h; Ambient temperature;
DOI:10.1039/P19890000827

Reference yield:

: 873-73-4
4-n-chlorophenylacetylene

: 123549-80-4
5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / 20 h

2: 82 percent / CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;
DOI:10.1039/P19890000827

Reference yield:

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 123549-80-4
5-(p-chlorophenyl)-3-mesitylisoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / 20 h

2: 82 percent / CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;
DOI:10.1039/P19890000827