Technology Process of 2-(5-phenylbenzoxazol-2-yl)phenol
There total 5 articles about 2-(5-phenylbenzoxazol-2-yl)phenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium pivalate; silver carbonate; Trimethylacetic acid;
In
N,N-dimethyl-formamide;
at 140 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/anie.201507272
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / methanol; chloroform / 20 °C / Inert atmosphere
2: sodium carbonate / ethyl acetate; water / 2 h / 0 °C / Inert atmosphere
3: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; Trimethylacetic acid; cesium pivalate; silver carbonate / N,N-dimethyl-formamide / 24 h / 140 °C / Inert atmosphere; Schlenk technique
With
silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium carbonate; hydrazine hydrate; cesium pivalate; silver carbonate; Trimethylacetic acid;
In
methanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.201507272
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve; Inert atmosphere
2: hydrazine hydrate / methanol; chloroform / 20 °C / Inert atmosphere
3: sodium carbonate / ethyl acetate; water / 2 h / 0 °C / Inert atmosphere
4: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; Trimethylacetic acid; cesium pivalate; silver carbonate / N,N-dimethyl-formamide / 24 h / 140 °C / Inert atmosphere; Schlenk technique
With
pyridine; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium carbonate; hydrazine hydrate; cesium pivalate; silver carbonate; copper(l) chloride; Trimethylacetic acid;
In
methanol; chloroform; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201507272
