(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

Base Information

Chemical Name:(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride
CAS No.:1365993-31-2
Molecular Formula:C₁₂H₅BrCl₂F₂N₂
Molecular Weight:365.992
Hs Code.:

Synonyms:(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

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Chemical Property of (Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

Chemical Property:

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Technology Process of (Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

There total 2 articles about (Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365993-01-6
N-(3-bromo-5-fluoropyridin-4-yl)-2-chloro-6-fluorobenzamide

: 1365993-31-2
(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

Guidance literature:: With thionyl chloride; In 1,2-dichloro-ethane; for 116h; Reflux; Inert atmosphere;

Reference yield:

: 79455-63-3
2-chloro-6-fluorobenzoyl chloride

: 1365993-31-2
(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 0 - 20 °C

1.3: 16 h / 20 °C

2.1: thionyl chloride / 1,2-dichloro-ethane / 116 h / Reflux; Inert atmosphere

With thionyl chloride; sodium hydride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1365993-31-2
(Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride

: 1365993-02-7
7-bromo-2-(2-chloro-6-fluorophenyl)thiazolo[5,4-c]pyridine

Guidance literature:: (Z)-N-(3-bromo-5-fluoro-4-pyridyl)-2-chloro-6-fluoro-benzimidoyl chloride; With pyridine; thiourea; In isopropyl alcohol; for 17h; Reflux;

With triethylamine; In isopropyl alcohol; for 1h; Reflux;