(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

Base Information

Chemical Name:(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide
CAS No.:1019852-78-8
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:

Synonyms:(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

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Technology Process of (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

There total 1 articles about (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (R)-2-methylbutan-1-amine hydrochloride

: 6190-46-1,89812-63-5
methyl (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)penta-2,4-dienoate

: 1019852-78-8
(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

Guidance literature:: (R)-2-methylbutan-1-amine hydrochloride; With trimethylaluminum; In toluene; benzene; at 0 - 20 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

methyl (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)penta-2,4-dienoate; In toluene; benzene; at 80 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/d0ob01745k

Reference yield:

: 1019852-78-8
(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide

: 36272-22-7
(R)-(+)-2-methylbutylamine

Guidance literature:: (2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)-N-((R)-2-methylbutyl)penta-2,4-dienamide; With hydrogenchloride; water; at 110 ℃;

With sodium hydroxide; In water; pH=10;
DOI:10.1016/j.bmc.2009.08.050