2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol

Base Information

• Chemical Name: 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol
• CAS No.: 1616253-64-5
• Molecular Formula: C₁₈H₂₆O
• Molecular Weight: 258.404

Synonyms:2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol

Chemical Property of 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol

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Technology Process of 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol

There total 1 articles about 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

(R)-5-isopropyl-2-methylcyclohexa-1,3-diene (4221-98-1) + 3,5-Dimethylphenol (108-68-9,50356-23-5) → 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol (1616253-64-5)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo5006069

Reference yield: 85.0%

trifluoromethylsulfonic anhydride (358-23-6) + 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol (1616253-64-5) → C19H25F3O3S (1627830-86-7)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; for 0.0833333h;

DOI:10.1021/jo5006069

Reference yield: 80.0%

2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylbenzene-1-ol (1616253-64-5) + acetic anhydride (108-24-7) → 2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylphenyl acetate (1616253-65-6)

Guidance literature:

With pyridine; at 80 ℃; Inert atmosphere;

DOI:10.1021/jo5006069

upstream raw materials:

(R)-5-isopropyl-2-methylcyclohexa-1,3-diene

3,5-Dimethylphenol

Downstream raw materials:

2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl pivalate

(1R,4R,5S,6S)-4-isopropyl-1-methyl-5-(2-methoxy-4,6-dimethylphenyl)oxabicyclo[4.1.0]heptane

(1R,4R,5S,6S)-4-isopropyl-1-methyl-5-(2-ethyl-4,6-dimethylphenyl)oxabicyclo[4.1.0]heptane

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