2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

Base Information

Chemical Name:2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate
CAS No.:1616253-72-5
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

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Chemical Property of 2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

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Technology Process of 2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

There total 4 articles about 2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1616253-65-6
2-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-3,5-dimethylphenyl acetate

: 1616253-72-5
2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo5006069

Reference yield:

: 4221-98-1
(R)-5-isopropyl-2-methylcyclohexa-1,3-diene

: 1616253-72-5
2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 3 h / 20 °C / Inert atmosphere

2: pyridine / 80 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere

With pyridine; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/jo5006069

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 1616253-72-5
2-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)-3,5-dimethylphenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 3 h / 20 °C / Inert atmosphere

2: pyridine / 80 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere

With pyridine; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/jo5006069