C₁₄H₁₁BO₃

Base Information

Chemical Name:C₁₄H₁₁BO₃
CAS No.:1222010-44-7
Molecular Formula:C₁₄H₁₁BO₃
Molecular Weight:238.051
Hs Code.:

C<sub>14</sub>H<sub>11</sub>BO<sub>3</sub>

Synonyms:C₁₄H₁₁BO₃

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Chemical Property of C₁₄H₁₁BO₃

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Technology Process of C₁₄H₁₁BO₃

There total 11 articles about C₁₄H₁₁BO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1222010-41-4
6-(1-phenyl-1-hydroxylmethyl)-1,3-dihydro-1-hydroxy-2,1-benzoxaborol

: 1222010-44-7
C₁₄H₁₁BO₃

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 59142-68-6
2-bromo-4-fluorobenzaldehyde

: 1222010-44-7
C₁₄H₁₁BO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

2.1: toluene-4-sulfonic acid / toluene / 96 h / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -80 °C / Inert atmosphere

3.2: 2 h

4.1: sodium tetrahydroborate / tetrahydrofuran; water / 3 h / 20 °C

5.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C

With sodium tetrahydroborate; n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 92161-30-3
5-benzoyl-2-bromomethylbromobenzene

: 1222010-44-7
C₁₄H₁₁BO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: N,N-dimethyl-formamide / 60 °C / Inert atmosphere

2.1: water; sodium hydroxide / methanol / 1 h / Reflux; Inert atmosphere

3.1: silica gel; pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / toluene / 96 h / Reflux; Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran / 0.58 h / -80 °C / Inert atmosphere

5.2: -80 - 20 °C / Inert atmosphere

5.3: 2 h / Inert atmosphere

6.1: sodium tetrahydroborate; water / tetrahydrofuran / 3 h / Inert atmosphere

7.1: silica gel; pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; water; silica gel; toluene-4-sulfonic acid; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;