(E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

Base Information

Chemical Name:(E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate
CAS No.:1142293-05-7
Molecular Formula:C₂₅H₃₄FNO₃Si₂
Molecular Weight:471.719
Hs Code.:

Synonyms:(E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

Suppliers and Price of (E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

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Technology Process of (E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

There total 1 articles about (E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1142293-03-5
(E)-Ethyl 3-(4-amino-3-fluorophenyl)-2-butenoate hydrochloride salt

: 125973-55-9
3,5-bis(trimethylsilyl)benzoic acid

: 1142293-05-7
(E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

Guidance literature:: With pyridine; trichlorophosphate; In acetonitrile; at 95 ℃; Inert atmosphere; Cooling with ice;

Reference yield: 49.0%

: 1142293-05-7
(E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate

: 1142292-56-5
(E)-3-[4-[[3,5-Bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoic acid

Guidance literature:: (E)-ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-3-fluorophenyl]-2-butenoate; With water; sodium hydroxide; In ethanol; at 50 ℃; for 1.5h;

With hydrogenchloride; In ethanol; water; at 20 ℃; Cooling with ice;