3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID

Base Information

Chemical Name:3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID
CAS No.:125973-55-9
Molecular Formula:C13H22O2Si2
Molecular Weight:266.487
Hs Code.:
Mol file:125973-55-9.mol

Synonyms:3,5-bis(4-aminophenyloxy)benzoic acid;Benzoic acid,3,5-bis(4-aminophenoxy);3,5-bis trimethylsilyl benzoic acid;3,5-bid(4-aminophenoxy)benzoic acid;3,5-Bis(4-aminophenoxy)benzoicacid;

Suppliers and Price of 3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,5-BIS-TRIMETHYLSILANYL BENZOIC ACID 95.00%
5MG
$ 502.90

Total 1 raw suppliers

Chemical Property of 3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID

Chemical Property:

Boiling Point:283.7±30.0 °C(Predicted)
PKA:4.28±0.10(Predicted)
PSA：37.30000
Density:0.98±0.1 g/cm3(Predicted)
LogP:2.47520

Purity/Quality:: 3,5-BIS-TRIMETHYLSILANYL BENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID

There total 4 articles about 3,5-BIS-TRIMETHYLSILANYL-BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 81500-98-3
3,5-bis(trimethylsilyl)acetophenone

: sodium hydrogensulfite

: 125973-55-9
3,5-bis(trimethylsilyl)benzoic acid

Guidance literature:: With potassium hydroxide; potassium carbonate; In water;

Reference yield: 33.0%

: 81500-98-3
3,5-bis(trimethylsilyl)acetophenone

: 125973-55-9
3,5-bis(trimethylsilyl)benzoic acid

Guidance literature:: With potassium hydroxide; calcium hypochlorite; potassium carbonate; In water; at 110 ℃; for 7.5h;
DOI:10.1021/jm00167a024

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 125973-55-9
3,5-bis(trimethylsilyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / Mg / tetrahydrofuran

2: 77 percent / AlCl₃ / CS₂ / 1 h / 0 °C

3: 33 percent / Ca(OCl)2, K₂CO₃, KOH / H₂O / 7.5 h / 110 °C

With potassium hydroxide; calcium hypochlorite; aluminium trichloride; potassium carbonate; magnesium; In tetrahydrofuran; carbon disulfide; water;
DOI:10.1021/jm00167a024