Technology Process of C20H18ClO2PS2
There total 3 articles about C20H18ClO2PS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H16ClO2PS2;
With
hexachloroethane; methyllithium;
In
tetrahydrofuran; diethyl ether;
at -60 ℃;
for 2h;
Inert atmosphere;
Schlenk technique;
methyl iodide;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/c3dt52800f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
1.2: 15 h / -78 - 20 °C
2.1: hexachloroethane; methyllithium / tetrahydrofuran; diethyl ether / 2 h / -60 °C / Inert atmosphere; Schlenk technique
2.2: 3 h / 20 °C / Inert atmosphere; Schlenk technique
With
n-butyllithium; hexachloroethane; methyllithium;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1039/c3dt52800f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methyllithium / tetrahydrofuran; diethyl ether / 1 h / 20 °C / Inert atmosphere; Schlenk technique
2.1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
2.2: 15 h / -78 - 20 °C
3.1: hexachloroethane; methyllithium / tetrahydrofuran; diethyl ether / 2 h / -60 °C / Inert atmosphere; Schlenk technique
3.2: 3 h / 20 °C / Inert atmosphere; Schlenk technique
With
n-butyllithium; hexachloroethane; methyllithium;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1039/c3dt52800f
