3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

Base Information

Chemical Name:3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide
CAS No.:1616732-45-6
Molecular Formula:C₆₃H₆₇Cl₄N₁₂O₁₀S*I
Molecular Weight:1453.08
Hs Code.:

3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

Synonyms:3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

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Chemical Property of 3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

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Technology Process of 3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

There total 7 articles about 3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1616732-42-3
3-(3-((prop-2-yn-1-ylcarbamoyl)oxy)propyl)-2-((1-(3-((prop-2-yn-1-ylcarbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)benzothiazol-3-ium iodide

: 1616732-44-5
N-(3-azidopropyl)-2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamide

: 1616732-45-6
3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

Guidance literature:: 3-(3-((prop-2-yn-1-ylcarbamoyl)oxy)propyl)-2-((1-(3-((prop-2-yn-1-ylcarbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)benzothiazol-3-ium iodide; With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; Inert atmosphere;

N-(3-azidopropyl)-2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamide; In water; N,N-dimethyl-formamide; at 100 ℃; for 0.05h; Reagent/catalyst; Solvent; Temperature; Microwave irradiation;

Reference yield:

: 91-22-5
quinoline

: 1616732-45-6
3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,4-dioxane / 2.5 h / Reflux

2.1: triethylamine / dichloromethane; methanol / Inert atmosphere; Reflux

3.1: dmap / dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C

3.2: 48 h / 0 - 20 °C

4.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / Inert atmosphere

4.2: 0.05 h / 100 °C / Microwave irradiation

With dmap; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 3-(3-hydroxypropyl)-2-methylbenzothiazol-3-ium iodide

: 1616732-45-6
3-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)-2-((1-(3-((((1-(3-(2-(2,3-dichloro-4-(2-methylenebutanoyl)phenoxy)acetamido)propyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoyl)oxy)propyl)quinolin-4(1H)-ylidene)methyl)beiizothiazol-3-ium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane; methanol / Inert atmosphere; Reflux

2.1: dmap / dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C

2.2: 48 h / 0 - 20 °C

3.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / Inert atmosphere

3.2: 0.05 h / 100 °C / Microwave irradiation

With dmap; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide;