N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine

Base Information

• Chemical Name: N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine
• CAS No.: 1334511-57-7
• Molecular Formula: C₄₆H₄₈N₂O₆S
• Molecular Weight: 756.963

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine

Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine

Chemical Property:

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine

There total 1 articles about N-(9-fluorenylmethoxycarbonyl)-O⁽³⁾-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-ethyl-S-triphenylmethyl-L-cysteine + O-tert-butyl-Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester (105751-13-1,244633-35-0) → N-(9-fluorenylmethoxycarbonyl)-O(3)-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine (1334511-57-7)

Guidance literature:

With 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In N,N-dimethyl-formamide; at 50 ℃; for 3h;

DOI:10.1039/c1ob05831b

Reference yield:

N-(9-fluorenylmethoxycarbonyl)-O(3)-tert-butyl-L-seryl-N-ethyl-S-triphenylmethyl-L-cysteine (1334511-57-7) + benzotriazol-1-ol (2592-95-2) → Fmoc-Ser(But)-(Et)Cys(Trt)-OBt

Guidance literature:

With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1002/psc.3290

upstream raw materials:

O-tert-butyl-N^α-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester

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