1-iodo-4-pentafluoroethylbenzene

Base Information

• Chemical Name: 1-iodo-4-pentafluoroethylbenzene
• CAS No.: 1265175-59-4
• Molecular Formula: C₈H₄F₅I
• Molecular Weight: 322.016
• Mol file: 1265175-59-4.mol

Synonyms:1-iodo-4-pentafluoroethylbenzene

Chemical Property of 1-iodo-4-pentafluoroethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1-iodo-4-pentafluoroethylbenzene

There total 1 articles about 1-iodo-4-pentafluoroethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pentafluoroethyl iodide (354-64-3) + 1,4-bromoiodobenzene (589-87-7) → 1-iodo-4-pentafluoroethylbenzene (1265175-59-4) + 1-bromo-4-(pentafluoroethyl)benzene

Guidance literature:

With copper; In dimethyl sulfoxide; at 150 ℃; for 1h; Microwave irradiation;

Reference yield: 49.0%

1-iodo-4-pentafluoroethylbenzene (1265175-59-4) + 3-(4-nitrophenyl)-1H-1,2,4-triazole (6219-52-9) → 3-(4-nitrophenyl)-1-(4-(pentafluoroethoxy)phenyl)-1H-1,2,4-triazole (1181214-80-1)

Guidance literature:

With 8-quinolinol; caesium carbonate; copper(l) iodide; In water; N,N-dimethyl-formamide; at 150 ℃; for 5h;

Reference yield:

1-iodo-4-pentafluoroethylbenzene (1265175-59-4) + 3-(4-methylphenyl)-1,2,4-triazole (23195-60-0) + 1-bromo-4-(pentafluoroethyl)benzene → 1-(4-Pentafluoroethyl-phenyl)-3-p-tolyl-1H-[1,2,4]triazole (1265175-56-1)

Guidance literature:

With copper(l) iodide; 8-quinolinol; caesium carbonate; In water; N,N-dimethyl-formamide; at 160 ℃; for 6h; Reflux;

upstream raw materials:

Pentafluoroethyl iodide

1,4-bromoiodobenzene

Downstream raw materials:

1-(4-Pentafluoroethyl-phenyl)-3-p-tolyl-1H-[1,2,4]triazole

3-(4-nitrophenyl)-1-(4-(pentafluoroethoxy)phenyl)-1H-1,2,4-triazole

Refernces

• 1、 -. "PESTICIDAL COMPOSITIONS". Page/Page column 31. . Retrieved 2011/02/24.