2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

Base Information

Chemical Name:2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole
CAS No.:1300713-17-0
Molecular Formula:C₁₅H₁₂N₄O₄S
Molecular Weight:344.351
Hs Code.:

Synonyms:2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

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Chemical Property of 2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

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Technology Process of 2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

There total 2 articles about 2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1127228-41-4
C₁₅H₁₄N₄O₄S

: 1300713-17-0
2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

Guidance literature:: With ammonium iron(III) sulfate; In methanol; at 80 ℃; for 1h;
DOI:10.1016/j.bmcl.2011.02.083

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 2131-61-5
p-nitrophenyl isothiocyanate

: 1300713-17-0
2-(3-methoxy-4-hydroxyphenyl)-5-(4-nitrophenylamino)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 1 h / 80 °C

2: ammonium iron(III) sulfate / methanol / 1 h / 80 °C

With ammonium iron(III) sulfate; hydrazine hydrate; In methanol;
DOI:10.1016/j.bmcl.2011.02.083