(3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane

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Chemical Name:(3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane
CAS No.:1104460-78-7
Molecular Formula:C₂₃H₃₃NO₇
Molecular Weight:435.518
Hs Code.:

Synonyms:(3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane

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Chemical Property of (3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane

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Technology Process of (3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane

There total 1 articles about (3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1104460-74-3
(3S,4'S,4''R,5'R)-2-benzyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-3,6-dihydro-2H-1,2-oxazine

: 108-24-7
acetic anhydride

: 1104460-78-7
(3R,4S,4'S,4''R,5'R)-2-acetyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-1,2-oxazinane

Guidance literature:: (3S,4'S,4''R,5'R)-2-benzyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-3,6-dihydro-2H-1,2-oxazine; With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 0.5h;

acetic anhydride; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol802514m