Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Base Information

Chemical Name:Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane
CAS No.:161584-76-5
Molecular Formula:C₂₄H₃₀N₂O₄Si
Molecular Weight:438.599
Hs Code.:

Synonyms:Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

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Technology Process of Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

There total 1 articles about Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 161584-82-3
Di(2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

: 161584-76-5
Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/jo00111a038

Reference yield: 85.0%

: 7677-24-9
trimethylsilyl cyanide

: 161584-76-5
Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

: Bis(6-cyano-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Guidance literature:: With N,N-Dimethylcarbamoyl chloride; In dichloromethane; 1.) r.t., 12 h, 2.) reflux;
DOI:10.1021/jo00111a038

Reference yield: 71.0%

: 626-05-1
2,6-Dibromopyridine

: 161584-76-5
Bis(1-oxo-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

: 49669-22-9
6,6'-Dibromo-2,2'-bipyridine

: (6-Bromo-pyridin-2-yl)-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-methanone

: 161584-87-8
Bis(6-bromo-2-pyridyl)<4-((tert-butyldimethylsilyl)oxy)phenyl>methanol

Guidance literature:: With n-butyllithium; In diethyl ether; Yield given; 1.) -78 deg C, 30 min, 2.) -78 deg C, 1 h; -78 deg C to r.t. 30 min, then r.t., 1 h;
DOI:10.1021/jo00111a038