5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

Base Information

Chemical Name:5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin
CAS No.:1450917-88-0
Molecular Formula:C₅₄H₄₂N₄O₂
Molecular Weight:778.953
Hs Code.:

Synonyms:5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

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Chemical Property of 5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

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Technology Process of 5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

There total 2 articles about 5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.8%

: 109-97-7,30604-81-0
pyrrole

: 109-63-7
boron trifluoride diethyl etherate

: 104-87-0
4-methyl-benzaldehyde

: 82-86-0
acenaphthene quinone

: 1450917-88-0
5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

Guidance literature:: pyrrole; boron trifluoride diethyl etherate; 4-methyl-benzaldehyde; acenaphthene quinone; In ethanol; chloroform; at 20 ℃; for 1h;

With chloranil; In ethanol; chloroform; for 2h; Reflux;

With triethylamine; In ethanol; chloroform; for 0.5h;
DOI:10.1142/S1088424613500673

Reference yield: 6.9%

: 109-97-7,30604-81-0
pyrrole

: 104-87-0
4-methyl-benzaldehyde

: 82-86-0
acenaphthene quinone

: 1450917-88-0
5-(8-ethoxycarbonyl-1-naphthyl)-10,15,20-tritolyl-porphyrin

Guidance literature:: pyrrole; 4-methyl-benzaldehyde; acenaphthene quinone; With boron trifluoride diethyl etherate; In ethanol; chloroform; at 20 ℃; for 1h;

With chloranil; In ethanol; chloroform; for 2h; Reflux;

With triethylamine; In ethanol; chloroform; for 0.5h;
DOI:10.1002/zaac.201300136