5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Base Information

Chemical Name:5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine
CAS No.:1542260-26-3
Molecular Formula:C₃₆H₄₄N₂O₈Si
Molecular Weight:665.8
Hs Code.:

Synonyms:5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Chemical Property:

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Technology Process of 5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

There total 2 articles about 5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.9%

: 1542260-21-8
5′-O-dimethoxytrityl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1542260-23-0
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 1542260-26-3
5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Guidance literature:: With pyridine; silver nitrate; In tetrahydrofuran; at 20 ℃; for 2.5h;

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 2′,3′,5′-trihydroxy-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 1542260-26-3
5′-O-dimethoxytrityl-3′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 4 h / 0 °C

2: silver nitrate; pyridine / tetrahydrofuran / 2.5 h / 20 °C

With pyridine; silver nitrate; In tetrahydrofuran;