C₁₅H₂₁NO₅

Base Information

Chemical Name:C₁₅H₂₁NO₅
CAS No.:943542-56-1
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:

C<sub>15</sub>H<sub>21</sub>NO<sub>5</sub>

Synonyms:C₁₅H₂₁NO₅

Suppliers and Price of C₁₅H₂₁NO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₅H₂₁NO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₅H₂₁NO₅

There total 25 articles about C₁₅H₂₁NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₃NO₆

: 943542-56-1
C₁₅H₂₁NO₅

Guidance literature:: With pyridine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/ol0706051

Reference yield:

: 943542-50-5
C₁₅H₂₃NO₆

: 943542-56-1
C₁₅H₂₁NO₅

Guidance literature:: Multi-step reaction with 13 steps

1.1: 8.8 g / t-BuOK / tetrahydrofuran / 6 h / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: tetrahydrofuran; methanol / 24 h / 20 °C

3.1: 3.9 g / NMO; TPAP / CH₂Cl₂ / 18 h / 20 °C

4.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

4.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

5.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

6.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

7.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

8.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

9.1: 53 percent / triethylamine / CH₂Cl₂ / 12 h / 20 °C

10.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

11.1: 66 mg / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 1.5 h / 0 °C

12.1: K₂CO₃; MeOH / 15 h / 20 °C

13.1: 42.5 mg / pyridine; BOPCl / acetonitrile / 2 h / 20 °C

With pyridine; 1.3-propanedithiol; hydrogenchloride; methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; potassium tert-butylate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol0706051

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 943542-56-1
C₁₅H₂₁NO₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrahydrofuran / 48 h / 20 °C

2.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

2.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

3.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

4.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

5.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

6.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

7.1: 53 percent / triethylamine / CH₂Cl₂ / 12 h / 20 °C

8.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

9.1: 66 mg / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 1.5 h / 0 °C

10.1: K₂CO₃; MeOH / 15 h / 20 °C

11.1: 42.5 mg / pyridine; BOPCl / acetonitrile / 2 h / 20 °C

With pyridine; 1.3-propanedithiol; hydrogenchloride; methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol0706051